TESTS

The Materials Analysis Laboratory (MAL) is an analytical laboratory for, the quality control of mineral raw materials, non-metallic inorganic materials and other industrial materials.

 

The diversity of the performed tests is one of the main differentiating factors of MAL, covering a wide range from the Characterization of materials to the Environmental and Industrial Hygiene Controls.

 

Within the accreditation scope of the laboratory are 62 accredited tests which cover the following technical areas:

  • Aggregates and Inerts
  • Asbestos
  • Ambient Air
  • Concrete, cement and mortars
  • Gaseous effluents
  • Liquid effluents
  • Solid waste
  • Ceramics and glass

 

The laboratory guarantees solid technical competence, based on specialized and experienced human resources and offering a wide range of equipment. Our team is qualified for controlling the quality of several matrices, according to analysis methodologies described in national or international standards, or even through internally developed methodologies, duly validated.

 

Regarding Quality Control, MAL’s goal is the reliability of obtained results and actions of Internal and External Quality Control are developed, using the regular use of Certified Reference Materials and the continuous participation in various programs of international interlaboratory tests.

 

Quantitative chemical analysis of aggregates and concretes (EN.1744-1)
Evaluation of air pollutants in suspension in ambient air (dust, crystalline silica, asbestos fibers)
Determination of the heavy metal content, Particles, SO2, fluorides, chlorides and H2S in gaseous effluents
Determination of pH, Conductivity, Total Suspended Solids (SST), Chemical Oxygen Demand (CQO), Biochemical Oxygen Demand (CBO5), Fluorides, Sulfates, Chlorides in liquid effluents
Chemical characterization of waste, for landfill purpose (Dec. Law nº 183/2009)
Determination of the chemical composition of raw materials ( sands, carbonates, clays, feldspars, calcites, kaolins, dolomites, chromites, plasters, etc)
Determination of Pb, Cd, Cr (VI) and Hg in packages and package waste glass, covered by the directive 94/62/CE
Determination of the solubility lead and cadmium in products containing food (EN 1388-1, ASTM C 738, ISO 6486-1, ISO 7086-1)
Tests for the certification of crystal glass and sonorous.
Granulometric analysis of a wide range of powder materials, including natural and synthetic ceramic powders, pigments, metal powders and others
Determination of real density of powders and compacts
Differential thermal analysis and thermogravimetric
Dilatometric analysis
Technological tests: retraction determination, flexural strength and water absorption after drying and firing, of samples raw materials or ceramics composition
Identification of crystalline phases by X-ray diffraction
Characterization of thermal behavior of materials by heating microscopy (up to 1700ºC)

Reception and Preparation of samples

Mills of jaws, hammers, rings and planetarium
Centrifugal sample separator
Precision cutting machine
Cutting machine and preparation of thin blades
Sample polishing machines
Press for mounting hot resins
Semi-automatic press HERZOG
PERL’X induction furnace
Various Muffles and Calibrated Stoves

Materials physics

Serigraph 5100 Micromeritics
Coulter LS 230
Micromeritics Helium Pycnometer
STA 409 Nezsch Thermobalance
402 C Netzsch Dilatometer
DSC 404 Netzsch Calorimeter
TG 209 Netzsch Microbalance
Big house shell
Brookfield Viscometer
Gallemkamp Viscometer
RV 20 Haake Viscometer
Ford cup

Materials Structure and Microstructure

X-ray diffractometer
Microscope heating
Optical polarization microscope
Binocular Loupe
Refractometer
511 Erichsen Colorimeter

Materials Chemistry

X-Ray Fluorescence Spectrometer (PHILIPS PW 1480)
UV / VIS Spectrophotometer (PerkinElmer Lambda 3)
Atomic Absorption Spectrophotometer (PerkinElmer AA300 - Flame)
Atomic Absorption Spectrophotometer (PerkinElmer AA600 Graphite Chamber)
Hydride generator
pH/Ion Metter

 

CONTACT

Alice Oliveira
T. +351 239499214 | Tm. +351 965841605
aoliveira@ctcv.pt

 

 

Laboratory Accredited by IPAC according to reference standard EN ISO / IEC 17025: 2005

 

 

IPAC